Hydrothermal synthesis of MoS2 nanosheets films: Microstructure and formation mechanism research | |
Miao, Hui1,2; Hu, Xiaoyun1,2; Sun, Qian1; Hao, Yuanyuan1; Wu, Hao1; Zhang, Dekai1,2; Bai, Jintao1,2; Liu, Enzhou3; Fan, Jun3; Hou, Xun1,2,4; Hu, XY | |
作者部门 | 瞬态光学技术国家重点实验室 |
2016-03-01 | |
发表期刊 | MATERIALS LETTERS
![]() |
ISSN | 0167-577X |
卷号 | 166页码:121-124 |
产权排序 | 4 |
摘要 | MoS2 nanosheets films were successfully prepared by Ti foil assisted hydrothermal synthesis method (labeled as Ti-MoS2 nanosheets films). The downside and upside of the films showed different novel morphologies with nanosheets arranged regularly and flowerlike microspheres, respectively. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscope (TEM). X-ray diffraction patterns showed that the peaks along (002) planes made a wide shift from 14.2 degrees to 9.4 degrees compared to its standard position located at 14.2 degrees at the beginning of the hydrothermal process, then gradually returned back to its normal position with the hydrothermal treatment time going on. However, time was not the only element to influence the position of the main diffraction peaks, a relatively low hydrothermal treatment temperature could also lead to the diffraction peaks' shift. In addition, TEM images indicated that the nanosheets film with hydrothermal treatment time for 24 h had a good single-crystal structure. Otherwise, the formation mechanism was carefully discussed and a possible formation mechanism was proposed. (C) 2015 Elsevier B.V. All rights reserved. |
文章类型 | Article |
关键词 | Thin Films Crystal Growth Microstructure |
学科领域 | 数理科学和化学 |
WOS标题词 | Science & Technology ; Technology ; Physical Sciences |
DOI | 10.1016/j.matlet.2015.12.010 |
收录类别 | SCI ; EI |
语种 | 英语 |
WOS研究方向 | Materials Science ; Physics |
项目资助者 | National Natural Science Foundation of China(51372201 ; Shaanxi Provincial Natural Science Foundation(2015JM5159) ; Research Fund for the Doctoral Program of Higher Education(20136101110009) ; 21476183) |
WOS类目 | Materials Science, Multidisciplinary ; Physics, Applied |
WOS记录号 | WOS:000369061100032 |
引用统计 | |
文献类型 | 期刊论文 |
条目标识符 | http://ir.opt.ac.cn/handle/181661/27686 |
专题 | 瞬态光学研究室 |
通讯作者 | Hu, XY |
作者单位 | 1.NW Univ Xian, Sch Phys, Xian 710069, Peoples R China 2.NW Univ Xian, Natl Photoelect Technol & Funct Mat & Applicat Sc, Xian 710069, Peoples R China 3.NW Univ Xian, Sch Chem Engn, Xian 710069, Peoples R China 4.Chinese Acad Sci, Xian Inst Opt & Precis Mech, State Key Lab Transient Opt & Technol, Xian 710068, Peoples R China |
推荐引用方式 GB/T 7714 | Miao, Hui,Hu, Xiaoyun,Sun, Qian,et al. Hydrothermal synthesis of MoS2 nanosheets films: Microstructure and formation mechanism research[J]. MATERIALS LETTERS,2016,166:121-124. |
APA | Miao, Hui.,Hu, Xiaoyun.,Sun, Qian.,Hao, Yuanyuan.,Wu, Hao.,...&Hu, XY.(2016).Hydrothermal synthesis of MoS2 nanosheets films: Microstructure and formation mechanism research.MATERIALS LETTERS,166,121-124. |
MLA | Miao, Hui,et al."Hydrothermal synthesis of MoS2 nanosheets films: Microstructure and formation mechanism research".MATERIALS LETTERS 166(2016):121-124. |
条目包含的文件 | ||||||
文件名称/大小 | 文献类型 | 版本类型 | 开放类型 | 使用许可 | ||
Hydrothermal synthes(1614KB) | 期刊论文 | 作者接受稿 | 限制开放 | CC BY-NC-SA | 请求全文 |
除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。
修改评论