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Hydrothermal synthesis of MoS2 nanosheets films: Microstructure and formation mechanism research
Miao, Hui1,2; Hu, Xiaoyun1,2; Sun, Qian1; Hao, Yuanyuan1; Wu, Hao1; Zhang, Dekai1,2; Bai, Jintao1,2; Liu, Enzhou3; Fan, Jun3; Hou, Xun1,2,4; Hu, XY
作者部门瞬态光学技术国家重点实验室
2016-03-01
发表期刊MATERIALS LETTERS
ISSN0167-577X
卷号166页码:121-124
产权排序4
摘要MoS2 nanosheets films were successfully prepared by Ti foil assisted hydrothermal synthesis method (labeled as Ti-MoS2 nanosheets films). The downside and upside of the films showed different novel morphologies with nanosheets arranged regularly and flowerlike microspheres, respectively. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscope (TEM). X-ray diffraction patterns showed that the peaks along (002) planes made a wide shift from 14.2 degrees to 9.4 degrees compared to its standard position located at 14.2 degrees at the beginning of the hydrothermal process, then gradually returned back to its normal position with the hydrothermal treatment time going on. However, time was not the only element to influence the position of the main diffraction peaks, a relatively low hydrothermal treatment temperature could also lead to the diffraction peaks' shift. In addition, TEM images indicated that the nanosheets film with hydrothermal treatment time for 24 h had a good single-crystal structure. Otherwise, the formation mechanism was carefully discussed and a possible formation mechanism was proposed. (C) 2015 Elsevier B.V. All rights reserved.
文章类型Article
关键词Thin Films Crystal Growth Microstructure
学科领域数理科学和化学
WOS标题词Science & Technology ; Technology ; Physical Sciences
DOI10.1016/j.matlet.2015.12.010
收录类别SCI ; EI
语种英语
WOS研究方向Materials Science ; Physics
项目资助者National Natural Science Foundation of China(51372201 ; Shaanxi Provincial Natural Science Foundation(2015JM5159) ; Research Fund for the Doctoral Program of Higher Education(20136101110009) ; 21476183)
WOS类目Materials Science, Multidisciplinary ; Physics, Applied
WOS记录号WOS:000369061100032
引用统计
被引频次:42[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.opt.ac.cn/handle/181661/27686
专题瞬态光学研究室
通讯作者Hu, XY
作者单位1.NW Univ Xian, Sch Phys, Xian 710069, Peoples R China
2.NW Univ Xian, Natl Photoelect Technol & Funct Mat & Applicat Sc, Xian 710069, Peoples R China
3.NW Univ Xian, Sch Chem Engn, Xian 710069, Peoples R China
4.Chinese Acad Sci, Xian Inst Opt & Precis Mech, State Key Lab Transient Opt & Technol, Xian 710068, Peoples R China
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Miao, Hui,Hu, Xiaoyun,Sun, Qian,et al. Hydrothermal synthesis of MoS2 nanosheets films: Microstructure and formation mechanism research[J]. MATERIALS LETTERS,2016,166:121-124.
APA Miao, Hui.,Hu, Xiaoyun.,Sun, Qian.,Hao, Yuanyuan.,Wu, Hao.,...&Hu, XY.(2016).Hydrothermal synthesis of MoS2 nanosheets films: Microstructure and formation mechanism research.MATERIALS LETTERS,166,121-124.
MLA Miao, Hui,et al."Hydrothermal synthesis of MoS2 nanosheets films: Microstructure and formation mechanism research".MATERIALS LETTERS 166(2016):121-124.
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